胡国忠, 朱杰琦, 朱健, 等. 微波辐射下页岩微结构的损伤特性与致裂效应[J]. 煤炭学报, 2020, 45(10): 3471-3479. DOI: 10.13225/j.cnki.jccs.2020.0209
引用本文: 胡国忠, 朱杰琦, 朱健, 等. 微波辐射下页岩微结构的损伤特性与致裂效应[J]. 煤炭学报, 2020, 45(10): 3471-3479. DOI: 10.13225/j.cnki.jccs.2020.0209
HU Guozhong, ZHU Jieqi, ZHU Jian, et al. Fracturing effect and damage behaviors for microstructure in shale under microwave irradiation[J]. Journal of China Coal Society, 2020, 45(10): 3471-3479. DOI: 10.13225/j.cnki.jccs.2020.0209
Citation: HU Guozhong, ZHU Jieqi, ZHU Jian, et al. Fracturing effect and damage behaviors for microstructure in shale under microwave irradiation[J]. Journal of China Coal Society, 2020, 45(10): 3471-3479. DOI: 10.13225/j.cnki.jccs.2020.0209

微波辐射下页岩微结构的损伤特性与致裂效应

Fracturing effect and damage behaviors for microstructure in shale under microwave irradiation

  • 摘要: 微波增产技术以其特有的加热特性、能源转换效率高和环保性,被认为是一种极具发展前景的页岩气开发新方法。为探索页岩气储层微波致裂改造的可行性与实效性,利用自主研制的微波辐射实验装置,开展了不同微波参量条件下页岩微波致裂实验;采用超声波法测定了微波辐射前、后页岩样的P波速度,研究了微波辐射下页岩微结构的损伤特性与破裂特征,初步探索了页岩微波致裂机制。结果表明:① 微波辐射下页岩温度快速升高且呈非均匀性分布,微波功率越大,非均匀性越强。② 微波辐射下页岩微结构损伤程度与微波功率、辐射次数、能量施加顺序以及页岩含水情况等因素相关。③ 相同微波能量作用下,完全饱水页岩的微结构数量增幅比干燥页岩要大。④ 页岩微结构演化存在微波能量阈值现象;相同微波能量作用下,随着辐射次数的增加,页岩微结构数量呈现“大幅增加→轻微增加→小幅增加”的趋势;相同辐射时间条件下,页岩微结构数量随着微波功率的递增总体上呈“轻微增加→大幅增加→小幅增加”的趋势,而其随着微波功率的递减则呈线性函数增加。⑤ 微波总能量小于120 kJ时,从小到大的能量施加顺序更有利于页岩微结构发育;微波总能量达到180 kJ时,页岩微结构发育对能量施加顺序不敏感。研究表明,微波辐射下页岩内所产生的热应力与蒸气压的共同作用,能使页岩内矿物晶体断裂、刚性矿物颗粒及颗粒界面产生微裂缝,引起页岩表面宏观裂缝发育,呈现显著的致裂效应,从而有利于提高页岩气储层渗透性。

     

    Abstract: Microwave stimulation technology is regarded as a promising new method for shale gas development due to its heating,high energy conversion efficiency and environmental friendly. Aimed at exploring the feasibility and effec- tiveness of microwave fracturing to shale,using the self-developed microwave irradiation device,we carried out some experiments on microwave fracturing to shale under different microwave parameters. The P-wave velocity of shale be- fore and after microwave radiation was tested with the ultrasonic method,for study the damage behaviors of microstruc- tures and fracturing characteristics of shale. And the microwave fracturing mechanism to shale was initially revealed. The results show that the temperature of shale under microwave irradiation increases rapidly and presents non-uniform distribution,and the higher the power,the stronger the non-uniformity. The damage degree of shale microstructure un- der microwave radiation is related to the microwave power,the irradiation times,the order of energy applying and the water saturation of shale. Under the same microwave energy,the number of microstructures of fully saturated shale in- creases more than that of dry shale. There are microwave energy threshold phenomena in the microstructure evolution and the macroscopic cracks development of shale samples. Under the same microwave energy,with the increase of radi- ation times,the number of shale microstructures shows a trend of significant increase,slight increase and smaller in- crease. Under the same irradiation time condition,the number of shale microstructures shows a trend of slight increase, significant increase and smaller increase,and it increases linearly with the decrease of microwave power. When the to- tal microwave energy is less than 120 kJ,the order of applying microwave energy from small to large is more favorable to the microstructure development of shale. When the total microwave energy reaches 180 kJ,the microstructure devel- opment of shale is not sensitive to the order of microwave energy application. This study indicates that the thermal stress and the vapour pressure in shale induced by microwave irradiation can cause the mineral chip breaking,lead the rigid particles and the particle interface in shale to produce microcracks,showing a significant fracturing effect. This is conducive to improving the permeability of shale gas reservoirs.

     

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