实时温度下煤系泥岩动态力学特性及微观破裂特征研究

Study on dynamic mechanical properties and microscopic fracture characteristics of coal measures mudstone at real-time temperature

  • 摘要: 我国露天煤矿普遍存在老窑采空区,区域内煤层自燃发火将对周围岩体的宏观力学特性及微观结构产生显著影响,爆破冲击载荷是诱发煤火燃烧区围岩失稳的关键因素,极易造成工作帮台阶崩塌、火灾等安全事故,对露天煤矿生产安全构成严重威胁。因此,开展实时温度下煤系泥岩动态力学特性及微观破裂机制研究,对露天煤矿工作帮台阶及安全开采具有重要意义。借助自主研制的高温分离式霍普金森压杆(H-SHPB)试验装置,开展常温(25 ℃)和实时温度100 、200 、300 、400 、500 ℃条件下煤系泥岩试样动态压缩试验,结合扫描电镜、能谱分析和组分测试试验,对煤系泥岩动态力学特性及宏细观断裂特征进行了系统的研究。研究结果表明:煤系泥岩动态峰值强度、弹性模量和峰值应变随应变率的增加而增大,表现出显著的应变率强化效应;固定应变率下,动态峰值强度和弹性模量随温度的增加呈现先增加后降低的变化趋势,在25~200 ℃温度区间呈波动上升趋势,200 ~500 ℃温度区间呈单调降低趋势;煤系泥岩破坏程度与应变率呈正相关,但其随温度增加表现为明显的区间效应;随应变率增加,煤系泥岩破坏后断口形貌逐渐由剪切断裂形貌向拉伸断裂形貌转化,且在高应变率下,钠长石和正长石晶粒骨架的破坏模式由沿晶破坏逐渐转变为穿晶破坏模式,这是煤系泥岩破坏程度增大的主要原因;温度对煤系泥岩的影响可分为2个阶段,25~200 ℃下煤系泥岩内部黏土矿物受热膨胀,填补骨架颗粒与黏土矿物间的空隙,使煤系泥岩整体更为密实,其破坏程度逐渐降低,表现为强化作用;200~500 ℃下煤系泥岩受高温热应力影响,内部裂隙增加,晶粒尺寸减小,导致其整体强度降低,破坏程度逐渐增加,表现为劣化作用。

     

    Abstract: In China's open-pit coal mines, there are generally goaf areas with old kilns. The spontaneous combustion of coal seams in the area will have a significant impact on the macroscopic mechanical properties and microscopic structure of the surrounding rock mass. The impact load of blasting is a key factor inducing the instability of the surrounding rock in the coal fire combustion area, which is prone to causing safety accidents such as collapse of working benches and fires, posing a serious threat to the production safety of open-pit coal mines. Therefore, conducting research on the dynamic mechanical characteristics and micro fracture mechanism of coal bearing mudstone under real-time temperature is of great significance for the working steps and safe mining of open-pit coal mines. With the help of the self-developed high-temperature separated Hopkinson pressure bar (H-SHPB) testing device, dynamic compression tests of coal bearing mudstone samples were carried out at room temperature (25 ℃) and real-time temperatures of 100, 200, 300, 400, and 500 ℃. Combined with scanning electron microscopy, energy spectrum analysis, and component testing experiments, the dynamic mechanical properties and macroscopic and microscopic fracture characteristics of coal bearing mudstone were systematically studied. The research results indicate that the dynamic peak strength, elastic modulus, and peak strain of coal bearing mudstone increase with the increase of strain rate, exhibiting a significant strain rate strengthening effect; Under a fixed strain rate, the dynamic peak strength and elastic modulus show a trend of first increasing and then decreasing with the increase of temperature, fluctuating upwards in the temperature range of 25−200 ℃, and monotonically decreasing in the temperature range of 200 ℃ to 500 ℃; The degree of damage to coal bearing mudstone is positively correlated with strain rate, but it exhibits a significant interval effect with increasing temperature; as the strain rate increases, the fracture morphology of coal bearing mudstone after failure gradually transforms from shear fracture morphology to tensile fracture morphology. Moreover, at high strain rates, the failure mode of sodium feldspar and orthoclase grain skeletons gradually changes from intergranular failure to transgranular failure mode, which is the main reason for the increase in the degree of damage of coal bearing mudstone; The effect of temperature on coal bearing mudstone can be divided into two stages. At 25−200 ℃, the clay minerals inside the coal bearing mudstone expand due to heat, filling the gaps between skeleton particles and clay minerals, making the coal bearing mudstone more compact as a whole. The degree of damage gradually decreases, showing a strengthening effect; Under the influence of high temperature thermal stress at temperatures between 200 and 500 ℃, coal bearing mudstone experiences an increase in internal cracks and a decrease in grain size, resulting in a decrease in overall strength and a gradual increase in degree of damage, exhibiting a deterioration effect.

     

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