液氮循环冷冲击煤体孔裂隙结构演化的多重分形特征

Investigation of multifractal features in coal pore-fracture network evolution induced by cyclic cryogenic liquid nitrogen shock

  • 摘要: 为探究液氮循环冷冲击对煤体孔裂隙结构的影响,开展不同循环次数(5、10、15、20次)液氮冷冲击致裂煤体试验。采用大尺寸核磁共振分析仪测试获得了循环冷冲击煤样T2谱以及核磁共振成像。引入多重分形理论对冷冲击次数煤体T2谱与核磁共振成像的非均匀演化特征进行量化评估,基于斯皮尔曼相关性分析建立循环次数与多重分形特征参数变化量的量化关系,从而揭示液氮循环冷冲击作用煤体孔裂隙结构非均匀演化特征。结果表明:液氮循环冷冲击处理显著改变了煤体孔裂隙结构,表现出非线性饱和特征。低循环次数(5~10次)时,孔隙率增量由1.76%快速提至2.05%。随循环次数的增加(10~20次),损伤逐渐累积使微小孔隙相互贯通形成较大孔裂隙,孔隙率增量放缓由2.05%提升至2.13%。核磁共振成像揭示了煤体内孔裂隙非均匀分布的特征,循环冷冲击作用下新生孔裂隙主要沿原始孔隙扩展,孔隙发育区域更易发生贯通性损伤,形成局部条带状高渗透通道,使煤样孔隙连通性增强。T2谱与核磁共振成像多重分形结果联合揭示了循环冷冲击作用下煤体孔裂隙非均匀演化特征,随循环次数增加,煤体内部孔径分布的均质性增强,但孔隙空间分布均质性降低。T2谱多重分形主要侧重于对样品内孔径大小和数量进行量化表征,核磁共振成像多重分形更侧重于对孔隙空间非均匀量化表征。构建了多重分形参量变化量与循环次数之间的拟合关系,直观揭示了循环冷冲击对煤体孔裂隙损伤作用的非线性饱和特性。对核磁共振曲线与核磁共振成像的多重分形特征参数进行综合分析可更直观地反映煤体内部孔裂隙非均匀动态演化规律,为液氮压裂现场施工参数设置提供数据支撑,对于施工参数优化具有指导意义。

     

    Abstract: To investigate the influence of cyclic liquid nitrogen cold-shock on coal pore-fracture evolution, specimens underwent cold-shock treatments at varying cycles (5, 10, 15, 20). Large-scale nuclear magnetic resonance (NMR) analysis provided T2 spectra and imaging of treated samples. Multifractal theory was applied to quantify heterogeneous evolution in T2 distributions and NMR image intensity with increasing cycles. Spearman correlation analysis established relationships between cycle number and multifractal parameter variations, revealing structural heterogeneity progression. Results indicate cyclic liquid nitrogen exposure induces nonlinear, saturation-characteristic alterations to coal pore-fracture networks. During initial cycles (5–10), porosity increased sharply from 1.76% to 2.05%. Subsequent cycles (10–20) promoted cumulative damage propagation wherein micropores coalesced into macroscale fractures, reducing porosity increment to 2.05%–2.13%. NMR imaging reveals the characteristics of non-uniform distribution of pores and fissures in coal. Under the action of cyclic cold shock, the new pores and fissures mainly expand along the original pores, and the pore development area is more prone to connectivity damage, forming a local banded high permeability channel, which enhances the pore connectivity of coal samples. The non-uniform evolution characteristics of pores and fissures in coal under the action of cyclic cold shock are revealed by the combination of T2 spectrum and multi-fractal results of nuclear magnetic resonance imaging. With the increase of the number of cycles, the homogeneity of pore size distribution in coal increases but the homogeneity of pore space distribution decreases. The T2 spectrum multifractal mainly focuses on the quantitative characterization of the pore size and number in the sample, and the nuclear magnetic resonance imaging multifractal focuses on the non-uniform quantitative characterization of the pore space. The fitting relationship between the change of multifractal parameters and the number of cycles is constructed, and the nonlinear saturation characteristics of the damage effect of cyclic cold shock on the pore and fracture of coal body are intuitively revealed. This integrated multifractal approach reveals dynamic heterogeneity in coal pore-fracture systems, providing data-driven support for optimizing field parameters in liquid nitrogen fracturing operations.

     

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