煤吸附甲烷结构变形的多尺度特征研究

Multi-scale characteristics of coal structure deformation during methane adsorption

  • 摘要: 通过扫描电镜对细观无烟煤样表面结构进行观测,研究了由结构镜质体与细观裂隙引起的煤体细观结构多尺度非均质特征;对比煤样表面CT扫描测试与分析结果,证实了不同尺度下煤体细观结构非均质特征与密度非均匀分布的一致性,即,在较小尺度下,由于煤中结构镜质体与细观裂隙结构的多样性,煤的细观结构和密度分布非均匀性很强,随着尺度的增大,煤的细观结构非均质特征减弱,密度分布非均匀性也减弱。通过对不同吸附压力下煤吸附甲烷CT扫描的数据进行多尺度三维分割与统计,揭示了煤吸附甲烷后细观结构膨胀/挤压变形与密度分布的相关性随结构尺度变化的规律;在小尺度上,低密度结构容易被挤压,中密度结构膨胀和挤压变形同时存在,高密度结构易于发生膨胀变形。随着煤结构尺度的增大,变形方式与原始结构密度的相关性降低。通过对不同尺度与吸附压力下的煤结构膨胀/挤压变形量、膨胀/挤压变形体积统计与分析,发现在甲烷吸附过程中,煤结构的膨胀变形和挤压变形均随结构尺度的增加而减小。煤的膨胀变形主要受吸附压力和结构尺度的影响,而挤压变形主要受结构尺度的单一因素的影响;煤中挤压变形体积始终小于膨胀变形体积。煤体结构的膨胀变形量与挤压变形量随尺度增加的衰减过程是非同步的,在小尺度下,煤体结构的挤压变形量比膨胀变形量更大,随着尺度增加,挤压变形量衰减速度比膨胀变形量衰减速度更快。研究结果对于煤层气开采过程中的气体渗流特征的多尺度精准动态评提供借鉴。

     

    Abstract: The surface structure of meso-anthracite samples was observed by scanning electron microscope ( SEM). The multi-scale heterogeneity characteristics of meso-structure of coal caused by the diversity of the mesopores and fractures in the vitrinite were studied. Comparing the results of CT scanning test and the analysis of coal sample sur- face,it is found that the heterogeneity of the meso-structures and the density distribution of anthracite is strong due to the diversity of the meso-pores and fractures in the vitrinite in the small scale. With the scale increase,the heterogeneity of the meso-structures and the density distribution of anthracite becomes weak. Through multi-scale three-dimension- al segmentation and the statistics of CT scan data of coal adsorbed methane under different adsorption pressures,the variation of the correlation between meso-structure swelling / extrusion deformation after coal adsorbed methane and density distribution with structure-scale change was revealed. Based on the statistics and analysis of swelling / extrusion deformation amount and volume of swelling / extrusion deformation of coal structure under different scales and adsorp- tion pressures,the main controlling factors of swelling and extrusion deformation in coal were revealed respectively. It is found that the volume of extrusion deformation is always smaller than that of the swelling deformation due to methane sorption. The attenuation process of swelling deformation and extrusion deformation of coal structures is asynchronous with the increase of scale. At small scale,the extrusion deformation of coal structure is larger than that of swelling de- formation. With the increase of scale,the attenuation rate of extrusion deformation is faster than that of swelling deform- ation. This study has an important theoretical value for the accurate and dynamic evaluation of multi-scale gas seepage characteristics in the process of coalbed methane exploitation.

     

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