液氮浸融对不同预制温度煤体损伤特性试验研究

Effect on liquid nitrogen impregnation of pore damage characteristics of coal at different temperatures

  • 摘要: 为研究液氮对不同预制温度煤体浸融后的表面裂隙扩展规律和孔隙损伤特性,分别采用显微镜观测、超声波波速测试以及核磁共振测试技术对不同预制温度煤体液氮浸融前后其表面裂隙扩展规律、内部微裂隙发育规律、内部孔隙发育过程及孔径分布变化规律进行试验研究。试验结果表明,液氮浸融过程中随着预制温度的升高,煤体表面产生热应力随之增大,煤体特征裂隙面积增比也随之增大,且热应力增加与煤表面特征裂隙面积增比呈显著相关关系。煤体预制温度越高液氮浸融后煤体内部超声波波速下降越明显,且煤体孔隙度增比越大,微裂隙、孔隙发育越良好。液氮浸融过程中煤体孔裂隙发育存在两个阶段:第1阶段中,微小孔隙向中大孔隙的转化数量大于微小孔自身新生数量,表现为液氮浸融后煤体微小孔数量减少,中大孔数量增加。随着煤体预制温度升高变为第2阶段,微小孔隙新生数量大于其向中大孔隙的转化量,表现为液氮浸融煤体后全孔隙段孔隙数量均增加。液氮浸融不同预制温度煤体后其特征裂隙增比-声波波速变化率-孔隙度变化率3者之间存在正相关关系。以上结果表明,煤体预制温度因素对液氮浸融后煤体表面裂隙发育及孔隙损伤特性影响显著,且液氮浸融不同预制温度煤体其表面裂隙扩展和内部损伤呈正相关关系。

     

    Abstract: In order to study the fracture expansion law and the pore damage characteristics of different prefabricated temperature coal that has been immersed by liquid nitrogen,microscopic observation,ultrasonic wave velocity test and nuclear magnetic resonance (NMR) technique are used respectively to study the fracture expansion,internal microfracture development,internal pore development,and pore size distribution of coal before and after being immersed by liquid nitrogen. The experimental results show that the increasing prefabricated temperature leads to the increase of thermal stress and characteristic fracture area. In addition,there is a strong correlation between the thermal stress and the increase ratio of coal surface fissure area. The higher the prefabricated temperature is,the bigger the porosity increase ratio of the coal after immersion gets. During immersion,there are two stages in the development of coal pore fractures development. In the first stage,the conversion number of micro pores to the medium or large pores is greater than the number of new ones. In other words,the number of micro pores falls while the number of medium or large pores rises. As the prefabricated temperature increases,it moves to the second stage,which the number of newborn micro pores is greater than that the conversion to the medium or large pores. In other words,the number of all pores rises. This paper studies the relationship between the fracture expansion law and the internal damage of different prefabricated temperature coal that has been immersed by liquid nitrogen. As a consequence,it finds the positive correlation among the characteristic fracture increase ratio,sonic wave velocity change rate and porosity change rate. The above experimental results show that the prefabricated temperature of coal has a significant effect on the fracture development and pore damage characteristics of coal which has been immersed by liquid nitrogen. Furthermore,there is a positive correlation between the fracture expansion and the internal damage.

     

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